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1. Microwave chemistry 1.1. Introduction to microwave heating. As many researchers have already stated in numerous published papers, microwave irradiation (usually at the ISM – Industrial Scientific and Medical – frequency of 2.45 GHz) produces efficient internal heating for most chemical reactions, delivering energy exactly where it is needed, even under exothermic conditions.

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Electric field simulation for the reaction system inside the microwave reactor is performed using the dielectric loss coefficient of the reaction system obtained from the measurement. Obtaining information on the electromagnetic field, which is invisible to the eye, enables a better-optimized reactor design.

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Microwave-assisted chemical desulfurization experiment was conducted in a microwave reactor purchased from Sine Microwave Chemistry Technology Co.Ltd, (Shanghai, China). The operating frequency was maintained at 2.45 GHz, and a schematic diagram of microwave desulfurization reactor is shown in Fig. 1. Download : Download high-res image (127KB)

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